(一)常见反应现象表述
1
加料加热
A gentle reflux appeared throughout the addition.
The temperature was increased from 25 ℃ to 50 ℃ during the addition.
2
反应过程中或者降温有固体析出
Solid was precipitate out after 1h reaction.
The reaction mixture was cooled to -10℃ , and solid was precipitate out.
3
加料不溶解
XX was added to the mixture, and the resulting suspension was stirred for 2h.
4
加热溶解
The suspension was heated to 90℃ and stirred until all solid was dissolved.
5
反应变粘稠/变色
The reaction mixture became sticky after 2hrs reaction/stirring.
After 2hrs stirring, the mixture turned into black/brown/gray/yellow/red color.
(二)特殊结果叙述
1
无进一步处理
No further operation
2
统一和其他批次一起后处理
The work-up of this batch was together with the other batches that recorded in the following pages.
3
检测条件,不需要后处理
IPC check showed this condition is better/bad for this reaction. No further operation / screen reaction.